Nanocrystalline chromium-doped Al2O3 and MgAl2O4 products were synthesised by combustion method in the presence of urea. The powders were characterised by X-ray diffraction analysis (XRD), scanning electron microscopy (SEM), BET surface area analysis, induction coupled plasma analysis (ICP) and mapping energy dispersive X-ray analysis (EDX). Fluorescence properties of the products were investigated in order to find the applications in fluorescent sensor and in the production of transparent polycrystalline ceramic materials for laser and optical application.

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