Nickel nanoparticles synthesized from NiCl2·6H2O by hydrazine hydrate in mixed solvent of ethanol and water in the presence of hydroxypropylmethylcellulose (HPMC) as protective and stabilizing agents. The morphology and sizes of synthesized Ni nanoparticles were studied by field-emission-scanning-electron microscopy (FESEM). Structural properties of nanoparticles were examined by X-ray diffraction (XRD). The polymer stabilized Ni nanoparticles were characterized by Fourier-transform infrared (FTIR) spectroscopy. The magnetic measurement showed that the resultant Ni nanoparticles were ferromagnetic. Also, the saturation magnetization (MS), remanent magnetization (MR) and coercivity (MR) were observed to increase with decreasing temperature. The results of magnetic characterization showed that the magnetic properties of the HPMC stabilized Ni nanoparticles are quite different from those of the bared Ni nanoparticles. All the observed magnetic properties essentially reflected the very typical nanoparticle type nature. Consequently, the resulting Ni nanoparticles were found to be highly active and recyclable catalyst for Suzuki coupling reactions.
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http://dx.doi.org/10.1016/j.carbpol.2013.05.020 | DOI Listing |
Sci Rep
December 2024
Department of Pharmaceutical Chemistry, Dr. D. Y. Patil Institute of Pharmaceutical Sciences and Research, Pimpri, Pune, India.
The emergence of self-propelling magnetic nanobots represents a significant advancement in the field of drug delivery. These magneto-nanobots offer precise control over drug targeting and possess the capability to navigate deep into tumor tissues, thereby addressing multiple challenges associated with conventional cancer therapies. Here, Fe-GSH-Protein-Dox, a novel self-propelling magnetic nanobot conjugated with a biocompatible protein surface and loaded with doxorubicin for the treatment of triple-negative breast cancer (TNBC), is reported.
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December 2024
School of Medicine, Yichun University, Yichun, 336000, China.
Iron oxide nanoparticles (IONPs) have the potential to be utilized in a multitude of fields, including biomedicine. Consequently, the potential health risks associated with their use must be carefully considered. Most biosafety evaluations of IONPs have focused on examining the impact of the material's distinctive physicochemical attributes.
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December 2024
Department of Nano-Chemical Engineering, Faculty of Advanced Technologies, Shiraz University, Shiraz, Iran.
MXene-based (nano)materials have recently emerged as promising solutions for antibiotic photodegradation from aquatic environments, yet they are limited by scalability, stability, and selectivity challenges in practical settings. We formulated FeO-SiO/MXene ternary nano-photocomposites via coupled wet impregnation and sonochemistry approach for optimised tetracycline (TC) removal (the second most used antibiotic worldwide) from water using response surface methodology-central composite design (RSM-CCD). The photocatalysts containing various loading of FeO/SiO (5-45 wt%) on the MXene with a range of calcination temperatures (300-600 °C) via RSM optimisation were synthesised, characterised regarding crystallinity properties, surface morphology, binding energy, and light absorption capability, and analysed for TC degradation efficiency.
View Article and Find Full Text PDFEnviron Sci Pollut Res Int
December 2024
Department of Mechanical Engineering, K. Ramakrishnan College of Engineering, Samayapuram, Trichy, India.
Lubricants are pivotal in mitigating friction and wear between surfaces, ensuring seamless movement of solid objects. However, the predominant use of petroleum-based lubricants in the automotive and industrial ssectors raises substantial concerns for future energy security. The exploration of vegetable oils as an alternative lubricant in the automotive industry was motivated by the depletion of fossil fuels and escalating environmental concerns.
View Article and Find Full Text PDFEnviron Sci Pollut Res Int
December 2024
Biosystem Engineering Department, Tarbiat Modares University (TMU), Tehran, Iran.
Today, there are environmental problems all over the world due to the emission of greenhouse gasses caused by the combustion of diesel fuel. The excessive consumption and drastic reduction of fossil fuels have prompted the leaders of various countries, including Iran, to put the use of alternative and clean energy sources on the agenda. In recent years, the use of biofuels and the addition of nanoparticles to diesel fuel have reduced pollutant emissions, improved the environment, and enhanced the physicochemical properties of the fuel.
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