The nickel-catalysed hydroalkoxylation of butadiene is promoted by a nickel(0)/dppb catalyst (dppb = 1,4-bis(diphenylphosphino)butane; see scheme). By following this new synthetic procedure, alkylbutenyl ethers are readily obtained from an alcohol and 1,3-butadiene with exclusion of dimerisation and telomerisation products.
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Nickel-catalysed hydroalkoxylation reaction of 1,3-butadiene: ligand controlled selectivity for the efficient and atom-economical synthesis of alkylbutenyl ethers.
Chemistry
July 2013
UCCS (Unité de Catalyse et de Chimie du Solide), Université Lille Nord de France-ENSCL, BP 90108, 59652 Villeneuve d'Ascq, France.
The nickel-catalysed hydroalkoxylation of butadiene is promoted by a nickel(0)/dppb catalyst (dppb = 1,4-bis(diphenylphosphino)butane; see scheme). By following this new synthetic procedure, alkylbutenyl ethers are readily obtained from an alcohol and 1,3-butadiene with exclusion of dimerisation and telomerisation products.
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