N,N'-[2,2'-(Phenyl-aza-nedi-yl)bis-(ethane-2,1-di-yl)]dipicolinamide.

Acta Crystallogr Sect E Struct Rep Online

College of Chemistry and Chemical Engineering, Hainan Normal University, Haikou 571158, People's Republic of China.

Published: May 2013

The asymmetric unit of the title compound, C22H23N5O2, contains two independent mol-ecules with similar conformations; the terminal pyridine rings are oriented at dihedral angles of 23.99 (8) and 18.07 (8)° with respect to the central benzene ring in one mol-ecule and 28.99 (8) and 23.22 (8)° in the other. In the crystal, N-H⋯O and weak C-H⋯O hydrogen bonds link the mol-ecules into a three-dimensional supra-molecular structure. Weak inter-molecular C-H⋯π inter-actions are also observed in the crystal.

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http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3647871PMC
http://dx.doi.org/10.1107/S1600536813008696DOI Listing

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N,N'-[2,2'-(Phenyl-aza-nedi-yl)bis-(ethane-2,1-di-yl)]dipicolinamide.

Acta Crystallogr Sect E Struct Rep Online

May 2013

College of Chemistry and Chemical Engineering, Hainan Normal University, Haikou 571158, People's Republic of China.

The asymmetric unit of the title compound, C22H23N5O2, contains two independent mol-ecules with similar conformations; the terminal pyridine rings are oriented at dihedral angles of 23.99 (8) and 18.07 (8)° with respect to the central benzene ring in one mol-ecule and 28.

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