Starting from an easily available pyridinol derivative, a route to penta(2-thienyl)pyridine and related symmetrical compounds is reported. Key reactions are activation of the pyridine core and metal-catalyzed couplings proving the efficacy of these methods even in sterically highly encumbered systems. UV/vis and fluorescence spectra as well as first cyclovoltametric measurements of the synthesized novel thiophene-pyridine conjugates are reported.
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| http://dx.doi.org/10.1021/ol303231c | DOI Listing |
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