An efficient synthesis of 2-substituted benzothiazoles in the presence of FeCl3/Montmorillonite K-10 under ultrasound irradiation.

Ultrason Sonochem

College of Chemistry and Environmental Science, Hebei University, Key Laboratory of Chemical Biology of Hebei Province, Baoding 071002, PR China.

Published: March 2013

2-Substituted benzothiazoles have been synthesized via one-pot reaction from aromatic aldehydes and o-aminothiophenol in the presence of FeCl(3)/Montmorillonite K-10 in absolute methanol at 25-30°C under ultrasound irradiation. The remarkable advantages are an inexpensive and easily available reagent, a simple procedure, mild conditions, short reaction times and moderate to good yields.

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http://dx.doi.org/10.1016/j.ultsonch.2012.09.010DOI Listing

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