Inverse-micelle-encapsulated water formed in the two-phase Brust-Schiffrin method (BSM) synthesis of Au nanoparticles (NPs) is identified as essential for dialkyl diselenide/disulfide to react with the Au(III) complex in which the Se-Se/S-S bond is broken, leading to formation of higher-quality Au NPs.
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Inverse-micelle-encapsulated water-enabled bond breaking of dialkyl diselenide/disulfide: a critical step for synthesizing high-quality gold nanoparticles.
J Am Chem Soc
October 2012
Department of Chemistry, Georgetown University 37th and O Streets NW, Washington, D.C. 20057, USA.
Inverse-micelle-encapsulated water formed in the two-phase Brust-Schiffrin method (BSM) synthesis of Au nanoparticles (NPs) is identified as essential for dialkyl diselenide/disulfide to react with the Au(III) complex in which the Se-Se/S-S bond is broken, leading to formation of higher-quality Au NPs.
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