Elemental analysis by NMR.

J Magn Reson

Division of Chemistry, Graduate School of Science, Kyoto University, 606-8502 Kyoto, Japan.

Published: November 2012

We explore the possibility for elemental analysis by NMR. To keep the efficiency of the signal acquisition common for all spin species, we propose to fix the frequency and vary the magnetic field to cover the isotopes involved in a sample. We introduce constant-frequency receptivity for quantitative elemental analysis in the frequency-fixed NMR experiment. Field-variable NMR experiments are demonstrated using a cryogen-free superconducting magnet. In addition to elemental analysis in liquid solution, solid-state NMR under magic-angle spinning is also described.

Download full-text PDF

Source
http://dx.doi.org/10.1016/j.jmr.2012.09.004DOI Listing

Publication Analysis

Top Keywords

elemental analysis
16
analysis nmr
8
nmr
5
elemental
4
nmr explore
4
explore possibility
4
possibility elemental
4
nmr efficiency
4
efficiency signal
4
signal acquisition
4

Similar Publications

Want AI Summaries of new PubMed Abstracts delivered to your In-box?

Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!