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Convention Abstracts of National Medical Association 2021.

J Natl Med Assoc

June 2022

Clinical Professor of Medicine and Medical Oncology, Department of Medical Oncology, Director, Center to Eliminate Cancer Disparities, Associate Director, Diversity Affairs, Sidney Kimmel Cancer Center at Jefferson, 116th President of the National Medical Association, Philadelphia, Pennsylvania.

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A simple and rapid method was developed for the determination of tylosin A and desmycosin residues in honey. Aliquots of honey samples were dissolved in a concentrated solution of sodium acetate and the target analytes were subsequently extracted with acetonitrile. The resulting organic extract was chromatographed under aqueous normal phase (ANP) LC conditions using a bare silica stationary phase with acidified solutions of ammonium formate in both water and 5:95 water: acetonitrile as the mobile phases.

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