A new crystal of N-(acetamide) morpholinium (NAM) bromide has been prepared in methanol at room temperature and characterized by single crystal X-ray analysis, elemental analysis, GS-MS, FTIR, NMR((1)H,(13)C, DEPTH and HETCOR). The N-(acetamide) morpholinium crystallizes in the orthorhombic crystal system, Pnma with unit cell a=12.798(9) Å, b=7.222(5) Å, c=9.244(5) Å, β=90.00, V=854.4(9) Å(3), Z=4. The X-ray structure determination revealed that there are strong inner and intermolecular hydrogen bonds in the crystal.
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| http://dx.doi.org/10.1016/j.saa.2011.05.055 | DOI Listing |
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