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2-(3-Oxo-1,3-dihydro-isobenzofuran-1-yl)-phthalazin-1(2H)-one. | LitMetric

2-(3-Oxo-1,3-dihydro-isobenzofuran-1-yl)-phthalazin-1(2H)-one.

Acta Crystallogr Sect E Struct Rep Online

School of Chemistry and Environment, South China Normal University, Guangzhou 510006, People's Republic of China.

Published: April 2009

The reaction of 2-carboxy-benzaldehyde and hydrazine hydrate unexpectedly yielded the title compound, C(16)H(10)N(2)O(3), which comprises one phthalide ring, one phthalazine system and a chiral centre. The phthalide unit is almost perpendicular to the phthalazine system, forming a dihedral angle of 87.1 (3)°. The packing is governed by weak C-H⋯O hydrogen-bonding inter-actions, forming layers parallel to the ab plane.

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Source
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977671PMC
http://dx.doi.org/10.1107/S1600536809011970DOI Listing

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