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A combined ion-sputtering and electron-beam annealing device for the in vacuo postpreparation of scanning probes. | LitMetric

A combined ion-sputtering and electron-beam annealing device for the in vacuo postpreparation of scanning probes.

Rev Sci Instrum

Department of Earth and Environmental Sciences and Center for NanoScience (CeNS), Ludwig-Maximilians-University, Theresienstrasse 41, 80333 Munich, Germany.

Published: March 2011

We describe the setup, characteristics, and application of an in vacuo ion-sputtering and electron-beam annealing device for the postpreparation of scanning probes (e.g., scanning tunneling microscopy (STM) tips) under ultrahigh vacuum (UHV) conditions. The proposed device facilitates the straightforward implementation of a common two-step cleaning procedure, where the first step consists of ion-sputtering, while the second step heals out sputtering-induced defects by thermal annealing. In contrast to the standard way, no dedicated external ion-sputtering gun is required with the proposed device. The performance of the described device is demonstrated by SEM micrographs and energy dispersive x-ray characterization of electrochemically etched tungsten tips prior and after postprocessing.

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Source
http://dx.doi.org/10.1063/1.3556443DOI Listing

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