High efficiency multichannel collimator for structural studies of liquids and low-Z materials at high pressures and temperatures.

Rev Sci Instrum

Institut de Minéralogie et de Physique des Milieux Condensés, UMR CNRS 7590, Université Pierre et Marie Curie, Université Paris Diderot, Paris, France.

Published: February 2011

A high efficiency multichannel collimator (MCC) device has been developed at the high pressure beamline ID27 of the European Synchrotron Radiation Facility to drastically reduce the x-ray background from the sample environment in the Paris-Edinburgh press. The main technical difficulty, which resides in the minimum slits size achievable using the classical mono-bloc design, has been resolved using an original concept based on a set of independent slits. Then, a very small slit size of 50 μm was manufactured resulting in a great improvement of the signal to background ratio. In addition, the transfer function of the MCC has been measured using the x-ray diffusion signal of a metal doped glass and efficiently applied to correct the raw data. The potential of this new device is illustrated in two challenging examples: iron-sulfur liquid structures and C(60) polymerization process at high pressure and high temperature.

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http://dx.doi.org/10.1063/1.3551988DOI Listing

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