A facile hydrothermal method has been developed and shown to be effective for the preparation of TiO(2)-graphene nanocomposite. The as-prepared nanocomposite was characterized using FT-IR spectroscopy, powder X-ray diffraction (XRD) and scanning electron microscopy (SEM). The TiO(2)-graphene modified glassy carbon electrode (GCE) exhibited remarkable electron transfer kinetics and electrocatalytic activity toward the oxidation of dopamine (DA). Furthermore, the oxidation of common interfering agent such as ascorbic acid (AA) was significantly suppressed at this modified electrode, which resulted in good selectivity and sensitivity for electrochemical sensing of DA. These results demonstrate that the TiO(2)-graphene hybrid material has promising potential applications in electrochemical sensors and biosensors design.
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http://dx.doi.org/10.1016/j.colsurfb.2010.10.048 | DOI Listing |
Sci Adv
January 2025
Thomas Lord Department of Mechanical Engineering and Materials, Duke University, Durham, NC 27708, USA.
Precise and rapid disease detection is critical for controlling infectious diseases like COVID-19. Current technologies struggle to simultaneously identify viral RNAs and host immune antibodies due to limited integration of sample preparation and detection. Here, we present acoustofluidic integrated molecular diagnostics (AIMDx) on a chip, a platform enabling high-speed, sensitive detection of viral immunoglobulins [immunoglobulin A (IgA), IgG, and IgM] and nucleic acids.
View Article and Find Full Text PDFMikrochim Acta
January 2025
Jiangxi Provincial Key Laboratory of Improved Variety Breeding and Efficient Utilization of Native Tree Species 2024SSY04093, College of Forestry, East China Woody Fragrance and Flavor Engineering Research Center of NF&GA, Jiangxi Agricultural University, Nanchang, 330045, People's Republic of China.
A convenient method is proposed using a heat-treatable volatile template to prepare hierarchical porous biochar (HPB). Litsea cubeba leaves and ZIF-8 served as carbon source and volatile hard template, respectively. The good compatibility between ZIF-8 and biomass facilitated their uniform dispersion, and the thermal decomposition of ZIF-8 created abundant pores in the HPB.
View Article and Find Full Text PDFJ Phys Chem Lett
January 2025
Department of Chemistry and Biochemistry, The University of Alabama, Tuscaloosa, Alabama 35487, United States.
We report a Tuning Fork Scanning Electrochemical Cell Microscopy (TF-SECCM) technique for providing morphological and electrochemical information on single redox-active entities. This new operation configuration of SECCM utilizes an electrolyte-filled nanopipette tip mounted onto a tuning fork force sensor to obtain a precise tip-sample distance control and surface morphological mapping capabilities. Redox activities of regions of interest (ROIs) can be investigated by scanning electrode potential by moving the nanopipette to any target regions while maintaining the constant force engagement of the tip with the sample.
View Article and Find Full Text PDFAnal Chem
January 2025
Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, School of Petrochemical Engineering, Changzhou University, Changzhou 213164, China.
Designing alloys with intrinsic chirality for chiral analysis is an interesting subject, since most alloys are achiral. Here, a starfish-shaped AuCu alloy is facilely prepared through simultaneous reduction of chloroauric acid (HAuCl) and copper chloride (CuCl) by l-ascorbic acid (l-AA). The resultant AuCu alloy exhibits fascinating chirality due to the chiral lattice distortion generated in the alloy.
View Article and Find Full Text PDFMikrochim Acta
January 2025
Department of Chemistry, Indian Institute of Technology Palakkad, Palakkad, Kerala, 678557, India.
Compared with previous decades, healthcare has emerged as a key global concern in light of the recurrent outbreak of pandemics. The initial stage in the provision of healthcare involves the process of diagnosis. Countries worldwide advocate for healthcare research due to its efficacy and capacity to assist diverse populations.
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