In this paper a new type of Fast Field Cycling (FFC) Nuclear Magnetic Resonance (NMR) relaxometer with low power consumption (200W) and cycle to cycle field stability better than 10(-4) is described. The new high-permeability magnet was designed to allow for good magnetic field homogeneity and allows for the sample rotation around an axis perpendicular to magnetic field, operating with magnetic fields between 0 and 0.21T. The power supply of the new relaxometer was specially developed in order to have steady state accurate currents and allow for magnetic field switching times less than 3ms. Additional control circuits were developed and included to compensate the Earth magnetic field component parallel to the field axis and to compensate for parasitic currents. The main aspects of the developed circuits together with some calibrating experimental results using the liquid crystal compounds 5CB and 8CB are presented and discussed.
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http://dx.doi.org/10.1016/j.ssnmr.2010.07.001 | DOI Listing |
Chem Commun (Camb)
January 2025
Physics Department & Shanghai Key Laboratory of Magnetic Resonance, School of Physics and Electronic Science, East China Normal University, North Zhongshan Road 3663, Shanghai 200062, P. R. China.
This study employs a low-field NMR (LF-NMR) method to investigate Cr(VI) adsorption and reduction in solid-liquid systems, focusing on three cellulose-based amine adsorbents. NMR revealed the effects of molecular structure on adsorption and reduction processes, providing insights into adsorbent design and mass transfer advantages for high-performance Cr(VI) adsorbents.
View Article and Find Full Text PDFPhysiol Res
December 2024
Department of Physiology, Faculty of Medicine, Masaryk University, Brno, Czech Republic.
Myocardial remodelling involves structural and functional changes in the heart, potentially leading to heart failure. The deoxycorticosterone acetate (DOCA)/salt model is a widely used experimental approach to study hypertension-induced cardiac remodelling. It allows to investigate the mechanisms underlying myocardial fibrosis and hypertrophy, which are key contributors to impaired cardiac function.
View Article and Find Full Text PDFSoft Matter
January 2025
Department of Applied Mechanics and Biomedical Engineering, Indian Institute of Technology Madras, Chennai, 600036, Tamil Nadu, India.
Bioinspired shape-morphing soft magnetic actuators have potential applications in medicine, robotics, and engineering due to their soft body, untethered control, and infinite degrees of freedom. The shape programming of the soft magnetic actuators (consisting of soft ferromagnetic CI particles in a soft matrix) is an involved task, as it requires a moulding process severely limiting the capability to program complex shapes. The current study explores a shape programming technique that architects the particle pattern configuration in the actuator, mimicking the pattern found in the mould-programmed actuator, thereby eliminating the need for a mould and providing a greater capability of programming complex shapes.
View Article and Find Full Text PDFJ Mater Chem B
January 2025
Department of General Surgery, Heilongjiang Provincial Hospital, Harbin, China.
There has been considerable interest in the recent advances in synthetic micro/nanomotors in diverse biofluids due to their potential biomedical applications. However, the propulsion of existing micro/nanomotor platforms for delivery in the gastrointestinal (GI) tract is inefficient. Herein, we present a magnetically and chemically actuated micromotor-tableted pill that can be actively retained in the GI tract .
View Article and Find Full Text PDFLangmuir
January 2025
Research Focus Area for Chemical Resource Beneficiation, Catalysis and Synthesis Research Group, North-West University, 11 Hoffman Street, Potchefstroom 2522, South Africa.
This study investigates the surfactant properties and efficiency of linear and Guerbet-type amino acid surfactants. Utilizing a Wilhelmy plate method, we assessed the colloidal efficiency of these surfactants, with the lowest observed critical micelle concentration at 0.046 mmol L, significantly reducing surface tension to as low as 25.
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