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Efficient Production of Self-Assembled Bioconjugate Nanovaccines against O2 Serotype in Engineered .
Nanomaterials (Basel)
April 2024
State Key Laboratory of Pathogen and Biosecurity, Beijing Institute of Biotechnology, No. 20 Dongdajie Street, Fengtai District, Beijing 100071, China.
Nanoparticles (NPs) have been surfacing as a pivotal platform for vaccine development. In our previous work, we developed a cholera toxin B subunit (CTB)-based self-assembled nanoparticle (CNP) and produced highly promising bioconjugate nanovaccines by loading bacterial polysaccharide (OPS) in vivo. In particular, the O2 serotype vaccine showcased a potent immune response and protection against infection.
View Article and Find Full Text PDFMicrostructured layered-kagome BaCo(VO)(OH) with variable crystallite size: alternative synthetic route and comparison with nanostructured samples.
Dalton Trans
March 2023
Nantes Université, CNRS, Institut des Matériaux de Nantes Jean Rouxel, IMN, F-44000 Nantes, France.
Microplatelets of the layered-kagome compound BaCo(VO)(OH), which is the Co analogue of mineral vesignieite BaCu(VO)(OH), have been prepared with very high yield by hydrothermal reaction using synthetic karpenkoite CoVO(OH)·2HO as starting reagent. The Rietveld refinement of X-ray diffraction data indicates that CoVO(OH)·2HO is isostructural with martyite ZnVO(OH)·2HO. Two single-phased samples of microstructured BaCo(VO)(OH) have been characterized using powder X-ray diffraction, FT-IR and Raman spectroscopies, thermal analyses, scanning electron microscopy, energy-dispersive X-ray spectroscopy and magnetisation measurements.
View Article and Find Full Text PDFImproved Process for the Preparation of Naloxegol Oxalate, an Opiod Receptor Antagonist.
ACS Omega
January 2023
Department of Engineering Chemistry, A. U. College of Engineering (A), Andhra University, Visakhapatnam 530003, India.
The present article discloses an improved and robust commercial process of the modern medicine naloxegol oxalate, which is used to treat opioid-induced constipation. The synthesis originates from the easily available key starting material, viz., naloxone, and ends with the oxalate salt of naloxegol (a pharmaceutically acceptable salt).
View Article and Find Full Text PDFPutting High-Index Cu on the Map for High-Yield, Dry-Transferred CVD Graphene.
ACS Nano
January 2023
Department of Engineering, University of Cambridge, CambridgeCB3 0FA, United Kingdom.
Reliable, clean transfer and interfacing of 2D material layers are technologically as important as their growth. Bringing both together remains a challenge due to the vast, interconnected parameter space. We introduce a fast-screening descriptor approach to demonstrate holistic data-driven optimization across the entirety of process steps for the graphene-Cu model system.
View Article and Find Full Text PDFFrom mixed group 13 cations [M(AlCp*)] (M = Ga/In/Tl) to an Al cluster.
Chem Sci
October 2022
Albert-Ludwigs-Universität Freiburg, Institute for Inorganic and Analytical Chemistry, Freiburg Materials Research Center FMF Albertstraße 21 79104 Freiburg i. Br. Germany
AlCp*-complexes with transition metals have shown to be highly reactive and enable C-H or Si-H bond activation. Yet, complexes of AlCp* with low-valent main-group metals are scarce. Here, we report the syntheses of [M(AlCp*)][Al(OR)] (R = C(CF)) with M = Ga, In, Tl, which include the first covalent Al-In and Al-Tl bonds.
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