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An NMR Study of Biomimetic Fluorapatite - Gelatine Mesocrystals.
Sci Rep
October 2015
Max-Planck-Institut für Chemische Physik fester Stoffe, Nöthnitzer Str. 40, 01187 Dresden, Germany.
The mesocrystal system fluoroapatite-gelatine grown by double-diffusion is characterized by hierarchical composite structure on a mesoscale. In the present work we apply solid state NMR to characterize its structure on the molecular level and provide a link between the structural organisation on the mesoscale and atomistic computer simulations. Thus, we find that the individual nanocrystals are composed of crystalline fluorapatite domains covered by a thin boundary apatite-like layer.
View Article and Find Full Text PDFFluorapatite-gelatine nanocomposite superstructures: new insights into a biomimetic system of high complexity.
Chemphyschem
June 2010
Physikalische Chemie I, Technische Universität Darmstadt, Petersenstrasse 20, 64287 Darmstadt, Germany.
Hierarchical pattern of microfibrils in a 3D fluorapatite-gelatine nanocomposite: simulation of a bio-related structure building process.
Phys Chem Chem Phys
April 2009
Physikalische Chemie, Technische Universität Darmstadt Petersenstrasse 20, D-64287 Darmstadt, Germany.
The shape development of a biomimetic fluorapatite-gelatine nanocomposite on the mum scale is characterised by a fractal mechanism with the origin being intrinsically coded in a (central) elongated hexagonal-prismatic seed. The 3D superstructure of the seed is distinctively overlaid by a pattern consisting of gelatine microfibrils. The orientation of the microfibrils is assumed to be controlled by an intrinsic electrical field generated by the nanocomposite during development and growth of the seed.
View Article and Find Full Text PDF"Hidden" hierarchy of microfibrils within 3D-periodic fluorapatite-gelatine nanocomposites: development of complexity and form in a biomimetic system.
Angew Chem Int Ed Engl
March 2008
Max Planck Institute for the Chemical Physics of Solids, Nöthnitzer Strasse 40, 01187 Dresden, Germany.
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