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Microwave-Assisted Cobalt-Catalyzed Synthesis of Quinazolinones via Acceptorless Dehydrogenative Coupling under Neat Condition.
Chem Asian J
January 2025
Department of Chemistry, Jadavpur University, Kolkata, 700032, West Bengal, India.
Herein, we present a sustainable and atom-economical approach for the synthesis of quinazolinones via acceptorless dehydrogenative coupling (ADC) using earth-abundant Co-salt, (CoCl) as the catalyst under neat condition. This method is distinguished by its green credentials, like, solvent-free, microwave-assisted heating, cost-effective, use of renewable alcohols, and generating only H and water as byproducts. Remarkably, this protocol achieves quinazolinone synthesis without the need for external ligands, oxidants, or additional additives.
View Article and Find Full Text PDFExtraction of Penicillin G From Dairy Products Using Deep Eutectic Solvent/Alginate Beads Enhanced via Layered Double Hydroxides.
J Sep Sci
November 2024
School of Chemistry, College of Science, University of Tehran, Tehran, Iran.
A new nanocomposite based on alginate microbeads impregnated with novel strontium-aluminum layered double hydroxide (Sr-Al LDH) incorporated with choline chloride-urea deep eutectic solvent (ChCl-U DES) was introduced. The microbeads and LDH were characterized by adsorption/desorption isotherms, Fourier-transform infrared spectroscopy, SEM, and x-ray diffraction. The adsorbent was employed for determining penicillin G (PENG) using dispersive solid-phase extraction prior to HPLC analysis.
View Article and Find Full Text PDFMore than one pathway: ECMO training and credentialing.
Crit Care Resusc
September 2024
Department of Medicine, Division of Critical Care Medicine, Cooper University Hospital, Cooper University Medical School at Rowan University, Camden, NJ, USA.
Procedural sedation competencies: a review and multidisciplinary international consensus statement on knowledge, skills, training, and credentialing.
Br J Anaesth
September 2024
Department of Emergency Medicine, Loma Linda University, Loma Linda, CA, USA.
Article Synopsis
- Procedural sedation lacks standardized competencies and training programs across various practitioners and settings, leading to inconsistency in practices.
- The International Committee for the Advancement of Procedural Sedation aimed to establish a consensus on the essential competencies required for practitioners, utilizing a framework focused on Competency-Based Medical Education.
- Through literature review and iterative consensus-building, the committee identified core competencies related to knowledge, skills, and attitudes, and proposed a structured framework for training and credentialing in procedural sedation.
Cu(II) Coordination Polymers for the Selective Oxidation of Biomass-Derived Veratryl Alcohol in Green Solvents: A Sustainable Catalytic Approach.
Inorg Chem
October 2024
School of Chemical Sciences, National Institute of Science Education and Research (NISER), An OCC of Homi Bhabha National Institute, PO Bhimpur-Padanpur, Via Jatni, Khurda, Bhubaneswar 752050, Odisha, India.
Four air-stable one-dimensional copper(II) coordination polymers (-) with azide linkers were synthesized using tridentate NNS and NNN ligands. Single-crystal X-ray diffraction (XRD) analysis confirmed the molecular structures of , , and . In the presence of TEMPO, all four coordination polymers demonstrated effective catalytic activity for the selective aerobic oxidation of veratryl alcohol, a biomass model compound, under base-free conditions.
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