Synthesis of glycoluril catalyzed by potassium hydroxide under ultrasound irradiation.

Ultrason Sonochem

College of Chemistry and Environmental Science, Hebei University, Key Laboratory of Analytical Science and Technology of Hebei Province, Baoding 071002, PR China.

Published: January 2010

AI Article Synopsis

  • Glycolurils were synthesized using potassium hydroxide as a catalyst, achieving yields between 17% and 75% at a temperature of 40 degrees Celsius in ethanol (EtOH) while applying ultrasound irradiation.
  • This method offers significant benefits over traditional stirring techniques, including the use of milder reaction conditions.
  • It also allows for a shorter reaction time, making the synthesis process more efficient.

Article Abstract

Synthesis of the glycolurils catalyzed by potassium hydroxide was carried out in 17-75% yield at 40 degrees C in EtOH under ultrasound irradiation. Compared to the method using stirring, the main advantage of the present procedure is milder conditions and shorter reaction time.

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http://dx.doi.org/10.1016/j.ultsonch.2009.04.010DOI Listing

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