Purpose: To evaluate in vitro the solubility of the Epiphany endodontic filling material Epiphany (Pentron Clinical Technologies, Wallingford, CT) prepared with its resinous solvent.

Methods: The specimens were prepared in the following experimental conditions: (1) GI, epiphany without photoactivation; (2) GII, Epiphany prepared with resinous solvent without photoactivation; (3) GIII, Epiphany followed by photoactivation; and (4) GIV, Epiphany prepared with resinous solvent followed by photoactivation. Ten specimens of each group were obtained from Teflon molds with 80% reduction in volume of the specimen's dimensions based on American National Standard Institute/American Dental Association (ANSI/ADA) Specification No. 57. The samples were weighted and immersed in distilled water for 7 days. After this period, they were removed, dried, and weighed again. Solubility was calculated by using samples weight loss (%). The immersion liquid was evaluated through atomic absorption spectrometry.

Results: The sealers without photoactivation were statistically similar (p > 0.05) between themselves (GI = 6.93% and GII = 6.39%) and different from the uncured sealers, which were statistically different between themselves (p < 0.05) (GIII = 3.56% and GIV = 0.47%). Only the Epiphany sealer prepared with resinous solvent followed by photoactivation presented solubility values within ANSI/ADA requirements, liberating the following amounts of ions: 114.43 microg of Ca(2+)/mL, 2.4 microg of Mg(2+)/mL, 0.33 microg of Fe(2+)/mL, 0.11 microg of Zn(2+)/mL, 1.31 microg of Ni(2+)/mL, and 7.1 microg of Na(+)/mL.

Conclusion: The association of resinous solvent to the Epiphany sealer followed by photoactivation resulted in a filling material with low solubility and expressive liberation of calcium ions.

Download full-text PDF

Source
http://dx.doi.org/10.1016/j.joen.2009.01.021DOI Listing

Publication Analysis

Top Keywords

prepared resinous
20
resinous solvent
20
solvent photoactivation
12
solubility epiphany
8
epiphany endodontic
8
sealer prepared
8
epiphany
8
filling material
8
epiphany photoactivation
8
epiphany prepared
8

Similar Publications

Research of mesoporous silica loaded lignin to enhance the anti-corrosion and anti-weathering performance of epoxy surface.

Int J Biol Macromol

January 2025

Key Laboratory of Automobile Materials, Ministry of Education, and College of Materials Science and Engineering, Jilin University, Changchun 130025, China. Electronic address:

A new type of filler was added to epoxy resin to prepare a composite coating with excellent corrosion and weathering resistance. The simple synthesis process and nonpolluting raw materials of this filler contribute to the development of green chemistry. Specifically, lignin was encapsulated in mesoporous silica, the synergistic effect between the two resulted in the formation of lignin/mesoporous silica composite particles (MSN-L) with excellent ultraviolet (UV) resistance.

View Article and Find Full Text PDF

Background: Polymethyl methacrylate (PMMA) is ideal for denture bases but is prone to biofilm accumulation, leading to denture stomatitis (DS), often involving . Dimethylaminohexadecyl methacrylate (DMAHDM) and 2-methacryloyloxyethyl phosphorylcholine (MPC) are introduced into dental materials for their antimicrobial and protein-repellent properties. This study investigates the effects of incorporating dimethylaminohexadecyl methacrylate (DMAHDM) and 2-methacryloyloxyethyl phosphorylcholine (MPC) into heat-polymerized (HP) and 3D-printed (3DP) denture base resins on microbial adhesion and cytotoxicity.

View Article and Find Full Text PDF

The objective of the present work was to prepare hybrid epoxy composites with improved mechanical and thermal properties. The simultaneous use of two different modifiers in an epoxy resin was motivated by the expected occurrence of synergistic effects on the performance properties of the matrix. Such a hybrid composite can be used in more severe conditions and/or in broader application areas.

View Article and Find Full Text PDF

In this paper, alumina-modified wood liquefaction (AL-WP) was prepared by blending nano-alumina (AlO) into wood liquefaction phenolic resin (WP) using a co-blending method. Alumina-modified wood liquefaction protofilament fiber (AL-WPF) was obtained by melt-spinning, curing, and thermo-curing processes, which were followed by carbonization to obtain alumina-modified wood liquefaction carbon fiber (AL-WCF). This paper focuses on the enhancement effect of nano-alumina doping on the mechanical properties and heat resistance of wood liquefaction carbon fiber (WCF), explores the evolution of graphite microcrystalline structure during the high-temperature carbonization process, and optimizes the curing conditions of AL-WPF.

View Article and Find Full Text PDF

This paper experimentally investigates the impact response of composite laminates made with conventional and bio-based epoxy resin. Drop tower impact tests were conducted at varying energy levels, including repeated low-energy impacts, to evaluate perforation resistance. The laminates' residual strength and damage tolerance were assessed using the Damage Index (DI) and by analysing the resonance frequency variations through the Impulse Excitation Technique (IET).

View Article and Find Full Text PDF

Want AI Summaries of new PubMed Abstracts delivered to your In-box?

Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!