Electron-beam-induced deposition allows the creation of three-dimensional nanodevices within a scanning electron microscope. Typically the dimensions of the fabricated structure are from 20 nm to several micrometers. Until now the record for the smallest deposited feature in an SEM was 3.5 nm, measured by an indirect method. We have achieved a nanodot having a full width half-maximum of 2.8 +/- 0.3 nm, measured directly in the same microscope after deposition.
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http://dx.doi.org/10.1021/nl900717r | DOI Listing |
Beilstein J Nanotechnol
January 2025
Physics Institute, Goethe University Frankfurt, Max-von-Laue-Str. 1, 60438 Frankfurt am Main, Germany.
A fast simulation approach for focused electron beam induced deposition (FEBID) numerically solves the diffusion-reaction equation (continuum model) of the precursor surface on the growing nanostructure in conjunction with a Monte Carlo simulation for electron transport in the growing deposit. An important requirement in this regard is to have access to a methodology that can be used to systematically determine the values for the set of precursor parameters needed for this model. In this work we introduce such a method to derive the precursor sticking coefficient as one member of the precursor parameter set.
View Article and Find Full Text PDFMolecules
January 2025
Faculty of Chemistry, Nicolaus Copernicus University in Toruń, Gagarina 7, 87-100 Toruń, Poland.
We report the synthesis and characterization of new, user-friendly gold(I) [Au(μ-(NH)CCF)] coordination polymer and [AuCl(NH(NH=)CCF)] complex. These compounds were investigated for potential application as precursors in chemical vapor deposition (CVD) and focused electron/ion beam-induced deposition (FEBID/FIBID), which are additive methods to produce nanomaterials. Single-crystal X-ray diffraction, elemental analysis, and infrared spectroscopy were used to determine the complexes' composition and structure.
View Article and Find Full Text PDFJ Phys Condens Matter
November 2024
Institute of Applied Physics, Vienna University of Technology, Wiedner Hauptstr. 8-10/134, Wien, 1040, AUSTRIA.
The transition from planar (2D) to three-dimensional (3D) magnetic nanostructures represents a significant advancement in both fundamental research and practical applications, offering vast potential for next-generation technologies like ultrahigh-density storage, memory, logic, and neuromorphic computing. Despite being a relatively new field, the emergence of 3D nanomagnetism presents numerous opportunities for innovation, prompting the creation of a comprehensive roadmap by leading international researchers. This roadmap aims to facilitate collaboration and interdisciplinary dialogue to address challenges in materials science, physics, engineering, and computing.
View Article and Find Full Text PDFMicrosc Res Tech
November 2024
Key Laboratory of Automobile Materials Ministry of Education, School of Materials Science & Engineering, Electron Microscopy Center, International Center of Future Science, Jilin Provincial International Cooperation Key Laboratory of High-Efficiency Clean Energy Materials, Jilin University, Changchun, China.
It is known that the interaction between electron beam and material surface enables a variety of physical phenomena, which hold significant inspiration for functional application. Herein, the process of in situ surface exsolution was observed and documented for the basalt phase in the Chang'e-5 lunar samples via scanning electron microscopy. Energy dispersive x-ray spectroscopy analysis confirmed the main existence of metal oxides such as plagioclase and pyroxene.
View Article and Find Full Text PDFBeilstein J Nanotechnol
October 2024
Department of Nanometrology, Wrocław University of Science and Technology, Janiszewskiego 11/17, 50-370, Wrocław, Poland.
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