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En route to (S)-selective chemoenzymatic dynamic kinetic resolution of aliphatic amines. One-pot KR/racemization/KR sequence leading to (S)-amides. | LitMetric
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En route to (S)-selective chemoenzymatic dynamic kinetic resolution of aliphatic amines. One-pot KR/racemization/KR sequence leading to (S)-amides.

Lahssen El Blidi Malek Nechab Nicolas Vanthuyne Stéphane Gastaldi Michèle P Bertrand Gérard Gil

J Org Chem

Equipe Chimie Moléculaire Organique, LCP UMR 6264, Boite 562, Université Paul Cezanne, Faculté des Sciences St Jérôme, Avenue Escadrille Normandie-Niemen, 13397 Marseille Cedex 20, France.

Published: April 2009

A one-pot sequential process, involving a radical racemization and an enzymatic resolution, provides access to (S)-amides, from racemic amines, with ee and yields ranging from 78 to 94% and 58 to 80%, respectively.

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 Source
http://dx.doi.org/10.1021/jo900074wDOI Listing

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