AI Article Synopsis
- Advances in atomic resolution environmental transmission electron microscopy are detailed, emphasizing gas-solid reactions at extremely high temperatures (around 2000°C).
- Recent innovations enable dynamic real-time studies at the Angstrom level using specialized hot stages in aberration corrected setups.
- Data from Pt/Pd nanoparticles on carbon demonstrate an impressive resolution of 0.11 nm at 500°C or more, showcasing the potential for advanced materials studies.
Article Abstract
Advances in atomic resolution in situ environmental transmission electron microscopy for direct probing of gas-solid reactions, including at very high temperatures (approximately 2000 degrees C) are described. In addition, recent developments of dynamic real time in situ studies at the Angstrom level using a hot stage in an aberration corrected environment are presented. In situ data from Pt/Pd nanoparticles on carbon with the corresponding FFT/optical diffractogram illustrate an achieved resolution of 0.11 nm at 500 degrees C and higher in a double aberration corrected TEM/STEM instrument employing a wider gap objective pole piece. The new results open up opportunities for dynamic studies of materials in an aberration corrected environment.
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| http://dx.doi.org/10.1002/jemt.20668 | DOI Listing |
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