A polymeric sol-gel combustion method has been used to synthesize nanocrystalline hydroxyapatite (HA) powder from calcium nitrate and triethyl phosphate with the addition of NH(4)OH. The sol-gel combustion process generates phase-pure nanocrystalline HA powder, as characterized using Fourier transform infrared (FTIR), X-ray diffraction (XRD), and transmission electron microscopy (TEM). Sintering of the HA powder compact at 1200 degrees C for 2 h leads to a 93% theoretical dense ceramic body. This method offers an easy route for the preparation of phase-pure nanocrystalline HA powder.
Download full-text PDF |
Source |
|---|---|
| http://dx.doi.org/10.1007/s10856-008-3685-x | DOI Listing |
Publication Analysis
Top Keywords
Similar Publications
Zinc Doped Akermanite: A Promising Biomaterial for Orthopedic Application with Enhanced Bioactivity, Mechanical Strength, and Bacterial Study.
ACS Omega
January 2025
Department of Chemistry, School of Advanced Sciences, Vellore Institute of Technology, Vellore 632014, Tamil Nadu, India.
Incorporating zinc into biocompatible materials has been identified as a potential strategy for promoting bone regeneration and osteogenic activity during hard tissue regeneration. This work aimed to investigate the impact of zinc doping on the structure of akermanite, which was synthesized using the sol-gel combustion method, with the goal of improving the biological response. Powder XRD and FT-IR analysis confirmed the phase purity and the respective functional groups associated with Zn-doped akermanite.
View Article and Find Full Text PDFInsights into the photocatalytic removal of malachite green organic pollutant by highly efficient hard responsive BaCoDyFeO catalysts.
Sci Rep
January 2025
Department, School of Chips, Xi'an Jiaotong-Liverpool University, Taicang, Suzhou, 215400, China.
The widespread discharge of organic dyes into the wastewater from various industrial processes has develop a major environmental apprehension in the modern world. To tackle such environmental issues, we are synthesizing a novel catalyst of composition, BaCoDyFeO (x = y = 0.02-0.
View Article and Find Full Text PDFRobustic and hybrid cobalt doped BaFeO hexaferrites for the photocatalytic degradation of Congo Red for wastewater treatment.
Sci Rep
December 2024
School of Physics and Materials Science, Shoolini University, Solan, H.P., India.
The industrial sector faces a significant challenge in finding the highly effective and efficient treatments for harmful dye-based color effluents. In this study, pure and cobalt doped barium hexaferrite of chemical formula, BaCoFeO (x = 0-0.06) are made via sol-gel auto-combustion (SC) methodology.
View Article and Find Full Text PDFValence State and Catalytic Activity of Ni-Fe Oxide Embedded in Carbon Nanotube Catalysts.
Nanomaterials (Basel)
December 2024
School of Materials Science and Engineering, Pusan National University, Busan 46241, Republic of Korea.
The catalytic activity of Ni-Fe oxide embedded in CNTs was investigated in terms of valence states and active oxygen species. Ni-Fe oxides were prepared by the sol-gel combustion process, and Ni-Fe oxides embedded in CNT catalysts were synthesized by the catalytic chemical vapor deposition (CCVD) method. The lattice structure of the Ni-Fe oxide catalysts was analyzed, and the lattice distortion was increased with the addition of Fe.
View Article and Find Full Text PDFComparative data on different preparation methods of Ru/CeO catalysts for catalytic oxidation of chlorine-containing volatile organic compounds.
Data Brief
December 2024
Yueyang Xingchang Petrochemical Co., Ltd., Yueyang 414000, PR China.
Under industrial conditions, efficient catalytic oxidation of Chlorinated volatile organic compounds is an important challenge, not only because of the poisonous effect of Chlorinated volatile organic compounds on catalysts, but also because of their high reaction temperature, which has an adverse impact on industrialization. In a recent article ( Ru/CeO ) [1], we developed a strategy for preparing a simple and efficient monolithic catalyst for the catalytic combustion of chlorobenzene. Ru/CeO was loaded on the industrial support cordierite by a Sol-gel method.
View Article and Find Full Text PDFWant AI Summaries of new PubMed Abstracts delivered to your In-box?
Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!