Analysis of zone-melted ultra-pure organic compounds: a new quantitative differential thermal analysis method.

Talanta

Department of Neurobiology in Psychiatry, University of Maryland, Baltimore, Maryland, U.S.A.

Published: February 1967

A method for the rapid quantitative determination of impurities in ultra-pure organic compounds is described. It is based on the difference in slopes of the curves obtained when the difference in temperature between the sample and a reference shield is plotted against time. The results are compared with those obtained by thermal analysis.

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http://dx.doi.org/10.1016/0039-9140(67)80178-4DOI Listing

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