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Homochiral layered indium phosphonates: solvent modulation of morphology and chiral discrimination adsorption.
Dalton Trans
January 2025
State Key Laboratory of Coordination Chemistry, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210023, P. R. China.
Assembling chiral coordination polymers into nano/microflower structures may improve their performance in applications such as chiral recognition and separation. In this study, we chose a chiral metal phosphonate system, , In(NO)/-, -pempH [pempH = (1-phenylethylamino)methylphosphonic acid], and carried out systematic work on the self-assembly of this system in different alcohol/HO mixed solvents under solvothermal conditions. Enantiomeric compounds -, -[In(pempH)(μ-OH)(HO)](NO) (R-, S-1) were obtained showing dense layered structures, but their morphologies varied with alcohol solvent.
View Article and Find Full Text PDFMaleic Acid-Butanol Pretreatment to Enhance Cellulose Accessibility for Enzymatic Hydrolysis and Ethanol Production from Oil Palm Empty Fruit Bunch.
ACS Environ Au
January 2025
Department of Chemical Science and Engineering, Graduate School of Engineering, Kobe University, 1-1 Rokkodaicho, Nada-Ku, Kobe 657-8501, Japan.
Pretreatment of lignocellulosic biomass is crucial yet challenging for sustainable energy production. This study focuses on enhancing enzymatic accessibility of cellulose in oil palm empty fruit bunches by optimizing pretreatment parameters to improve glucose and ethanol yields while reducing fermentation inhibitors. It evaluates the impact of maleic acid concentrations on biorefinery processes.
View Article and Find Full Text PDFUrinary odor molecules in the Otassha Study can distinguish patients with sarcopenia: A pilot study.
Geriatr Gerontol Int
January 2025
Faculty of Life Sciences, Kyoto Sangyo University, Kyoto, Japan.
Aim: To identify sarcopenia markers in urinary odor.
Methods: We performed solid-phase microextraction from the headspace and gas chromatography-mass spectrometry analysis of urinary volatile organic compounds (VOCs) in 71 healthy individuals and 68 patients diagnosed with sarcopenia according to the Asian Working Group on Sarcopenia 2019 criteria. The mass-to-charge ratios (m/z) of 10 VOCs with a significant difference in the total ion chromatogram of 220 VOCs detected in this study were compared by U-test.
Sensing of -butanol vapours using an oxygen vacancy-enriched ZnSnO-SnO hybrid-composite.
Phys Chem Chem Phys
January 2025
Radiochemistry Division, Bhabha Atomic Research Centre, Trombay, Mumbai-400085, India.
The precise identification of various toxic gases is important to prevent health and environmental hazards using cost-effective, efficient, metal oxide-based chemiresistive sensing methods. This study explores the sensing properties of a chemiresistive sensor based on a ZnSnO-SnO microcomposite for detecting -butanol vapours. The microcomposite, enriched with oxygen vacancies, was thoroughly characterized, confirming its structure, crystallinity, morphology and elemental composition.
View Article and Find Full Text PDFDevelopment and validation of a rapid and accurate ultra performance liquid chromatography-photodiode array method for concurrent quantification of thirty-two polyphenols in edible fruit of Cordia myxa Linn.
J Chromatogr A
December 2024
Chemical Technology Division, CSIR-Institute of Himalayan Bioresource Technology, Palampur (Himachal Pradesh), 176061, India; Academy of Scientific and Innovative Research, (AcSIR), Ghaziabad, 201002, India. Electronic address:
The aim of current work was to develop a novel, simple, sensitive, and reliable method for screening and quantification of thirty-two polyphenol compounds from Cordia myxa (C. myxa) using Ultra Performance Liquid Chromatography Photodiode Array detector (UPLC-PDA). With the help of the quaternary solvent manager and a comparison study of seven different columns packed with silica particles that are less than two micron thick (1.
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