Complete NMR data assignments for novel pterocarpans from Harpalyce brasiliana.

Magn Reson Chem

Curso de Pós-Graduação em Química Orgânica, Departamento de Química Orgânica e Inorgânica, Universidade Federal do Ceará, Cx. Postal12200, 60.021-940, Fortaleza-CE, Brazil.

Published: September 2008

A NMR study of two new pterocarpans isolated from the roots of Harpalyce brasiliana is described. In addition to 1D NMR, 2D shift-correlated NMR pulse sequences ((1)H-(1)H-COSY, HSQC and HMBC) were used to establish the structures, and unambiguously perform the (1)H and (13)C chemical shift assignments.

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Source
http://dx.doi.org/10.1002/mrc.2269DOI Listing

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