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Expeditious microwave-assisted thionation with the system PSCl3/H2O/Et3N under solvent-free condition. | LitMetric

Expeditious microwave-assisted thionation with the system PSCl3/H2O/Et3N under solvent-free condition.

J Org Chem

Synthetic Chemistry Division, Defence Research & Development Establishment, Gwalior- 474002, India.

Published: April 2008

AI Article Synopsis

Article Abstract

A novel thionation protocol for carbonyl compounds, with the system PSCl3/H2O/Et3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation.

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Source
http://dx.doi.org/10.1021/jo7022069DOI Listing

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