p-Nitrobenzoyl tetramethylguanidine and m-nitrobenzoyl tetramethylguanidine were synthesized by simple methods. Their main IR and Raman spectra were measured, quantum-calculated, and assigned by the program Gaussian 98. The results showed that the theoretical spectra were in good agreement with the experimental ones, and can be used as a guidance in the interpretation of experimental spectra.
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