In the present study, the possibility of using leaky Rayleigh waves as a nondestructive tool for the evaluation of CVD diamond coating layer is explored experimentally. For this purpose, a set of CVD diamond coated specimens are prepared and the leaky Rayleigh waves are measured in an immersion, pulse-echo setup. For the proper analysis of the acquired signals we propose a novel signal analysis approach, namely the "time trace angular scan (TTAS)" image. Then, the proposed approach together with the backward radiation profiles are applied for the analysis of signals acquired in the initial experiments. The TTAS image shows the entire information on both time-of-arrival and angle of incidence of the signals for the proper "time-angle windowing." Then, the backward radiation profile of the windowed signals provides adequate parameters from which nondestructive evaluation of the coated specimens is carried out.
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http://dx.doi.org/10.1016/j.ultras.2006.05.053 | DOI Listing |
J Phys Chem A
December 2024
Skobeltsyn Institute of Nuclear Physics, Moscow State University, Leninskie gory, Moscow 119991, Russia.
An attenuation of visible probe radiation identified in earlier absorption studies of microwave plasma-activated CH/H/Ar gas mixtures is shown to arise from nanoparticles in under-pumped regions on opposing sides of a reactor used for diamond chemical vapor deposition. The present modeling studies highlight (i) ejection of Si-containing species into the gas phase by reactive radical etching of the quartz window through which the microwave radiation enters the reactor, enabled by suitably high window temperatures () and the synergistic action of near-window H atoms and CH radicals; (ii) subsequent processing of the ejected material, some of which are transported to and accumulate in stagnation regions in the entrance to the reactor side arms; and (iii) the importance of Si in facilitating homogeneous gas phase nucleation, clustering, and nanoparticle growth in these regions. The observed attenuation, its probe wavelength dependence, and its variations with changes in process conditions can all be rationalized by a combination of absorption and scattering contributions from Si/C/H containing nanoparticles with diameters in the range of 50-100 nm.
View Article and Find Full Text PDFAppl Radiat Isot
February 2025
Department of Physics, University of Surrey, Guildford, Surrey, GU2 7XH, UK.
In this project, we conducted micro-beam sensitivity mapping using the Diamond Light Source (DLS) synchrotron. We fabricated three samples with distinct metal contacts: Platinum (HPS-Pt) and Aluminium/Platinum (HPS-Al/Pt) on high-quality single crystal CVD diamond, and Platinum (VS-Pt) on lower purity single crystal CVD diamond. Our objective was to identify the most suitable sample for synchrotron measurements, particularly focusing on the lower purity sample due to its unique characteristics, such as thin nitrogen lines and substrate area.
View Article and Find Full Text PDFACS Appl Nano Mater
November 2024
Institute of Physics, Czech Academy of Sciences, Cukrovarnická 10/112, Prague 6 162 00, Czech Republic.
Nanodiamonds (NDs) containing optically active centers have gained significant relevance as the material of choice for biological, optoelectronic, and quantum applications. However, current production methods lag behind their real needs. This study introduces two CVD-based approaches for fabricating NDs with optically active silicon-vacancy (SiV) color centers: bottom-up (BU) and top-down (TD) methods.
View Article and Find Full Text PDFPolymers (Basel)
September 2024
Assembly and Engineering Metrology, Department of Machining, Faculty of Mechanical Engineering, Technical University of Liberec, 461 17 Liberec, Czech Republic.
Conventional dry machining (without process media) of carbon fibre composite materials (CFRP) produces tiny chips/dust particles that float in the air and cause health hazards to the machining operator. The present study investigates the effect of cutting conditions (cutting speed, feed per tooth and depth of cut) during CFRP milling on the size, shape and amount of harmful dust particles. For the present study, one type of cutting tool (CVD diamond-coated carbide) was used directly for machining CFRP.
View Article and Find Full Text PDFGenet Med
September 2024
Department of Biochemistry, Yong Loo Lin School of Medicine, National University of Singapore, Singapore; Immunology Program, Life Sciences Institute, National University of Singapore, Singapore; Singapore Lipidomics Incubator (SLING), Life Sciences Institute, National University of Singapore, Singapore; Cardiovascular Disease Research (CVD) Programme, Yong Loo Lin School of Medicine, National University of Singapore, Singapore; Immunology Translational Research Program, Yong Loo Lin School of Medicine, National University of Singapore, Singapore. Electronic address:
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