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| http://dx.doi.org/10.1042/bj0200483 | DOI Listing |
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Competition vs. Cooperativity of I···Omorpholinyl and I···Cl-M Halogen Bonds in Cocrystals of Zinc(II) and Copper(II) Coordination Compounds Carrying Multiple Acceptor Sites.
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In order to explore a strategy for synthesizing halogen-bonded metal-organic cocrystals by utilizing metal complexes whose pendant chloride group and the morpholinyl oxygen atom enables halogen bonding, we have synthesized four pentacoordinated Cu(II) and Zn(II) complexes of the MCl2L general formula (L=imines prepared by the condensation reaction of 4-aminoethylmorpholine with 2-pyridinecarboxyaldehide or 2-acetylpyridine). The prepared metal complexes were further cocrystallized with selected iodoperfluorinated benzenes. Out of 20 combinations, 14 experiments yielded crystals suitable for single-crystal X-ray diffraction.
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