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Cost-effective low-volume sample introduction system for open tubular capillary ion chromatography via a hybrid negative pressure approach.

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Open tubular capillary ion chromatography (OTIC) exhibits a minute sample/eluent volume separation with a low-pressure operation (<30 psi) and potentially develops for a portable analytical device. In this study, a novel and cost-effective low-volume sample-introduction system has been developed for the OTIC and applied for separating water-soluble small inorganic ions. This innovative design uses a hybrid negative pressure (HNP) system, considerably reducing sample consumption to ∼7 μL per injection while maintaining excellent repeatability (<4 % relative standard deviation) on a 50 μm bore capillary tube.

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The paper describes the results of experimental studies of media as an intermediary in heat exchange taking place in low volume conditions. Their properties predestine them both as a future-proof for transporting and storing heat materials. The paper concerns the current topic related to the miniaturization of cooling heat exchangers.

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