Ultrasound-assisted synthesis of 1,8-dioxo-octahydroxanthene derivatives catalyzed by p-dodecylbenzenesulfonic acid in aqueous media.

Ultrason Sonochem

Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding 071002, PR China.

Published: April 2006

An efficient and convenient approach to the synthesis of 3,3,6,6-tetramethyl-9-aryl-1,8-dioxo-octahydroxanthene derivatives using p-dodecylbenzenesulfonic acid (DBSA) as the catalyst (10 mol.%) under ultrasound irradiation is described. This method provides several advantages such as environment friendliness, high yields and simple work-up procedure. In addition, water was chosen as a green solvent.

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http://dx.doi.org/10.1016/j.ultsonch.2005.04.002DOI Listing

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