The influence of oxygen content in helium on the accuracy of nc/nH ratio determination for model mixtures of aliphatic and polyaromatic hydrocarbons and polychlorinated biphenyls was studied. The best accuracy was achieved at the oxygen content ca. 9%, which was the maximal possible oxygen content in helium for this GC-atomic emission detection (helium flow rate was 25 ml min(-1)). Using the maximal oxygen flow in plasma the nC/nH ratio determination accuracy improvement was accompanied by 10-fold increase in detection limit.
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| http://dx.doi.org/10.1016/j.chroma.2004.09.021 | DOI Listing |
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