Effect of solvent, temperature, and solvent-to-solid ratio on the total phenolic content and antiradical activity of extracts from different components of grape pomace.

J Agric Food Chem

Escuela Técnica Superior de Ingeniería, Universidad de Santiago de Compostela, Lope Gómez de Marzoa, 15782 Santiago de Compostela, Spain.

Published: March 2005

Grape byproducts were subjected to an extraction process under various different experimental conditions (namely, solvent type, temperature, solvent-to-solid ratio, time contact, and raw material) in order to study the effect of these conditions on the yield of phenolic compounds and the corresponding antiradical activity of extracts. Although the order of decreasing capacity to extract soluble materials was ethanol > methanol > water, methanol was the most selective for extracting phenolic compounds. Temperature and solvent-to-solid ratio were found to have a critical role in extraction efficiency; values of 50 degrees C (between 25 and 50 degrees C) and 1:1 (between 1:1 and 5:1) maximized the antiradical activity of phenolic extracts. In addition, extracts from grape samples previously subjected to distillation reached higher antiradical values in comparison to those coming directly from pressing; in both cases, seed extracts showed better results than those of stem when ethanol or water was employed, whereas the opposite occurred in the case of methanol. These differences were attributed to the different phenolic compositions of the considered fractions.

Download full-text PDF

Source
http://dx.doi.org/10.1021/jf0488110DOI Listing

Publication Analysis

Top Keywords

temperature solvent-to-solid
12
solvent-to-solid ratio
12
antiradical activity
12
activity extracts
8
phenolic compounds
8
phenolic
5
extracts
5
solvent temperature
4
ratio total
4
total phenolic
4

Similar Publications

Phenolic compounds have antiglycation activity, but the changes occurring during thermal treatment (TT) in these activities are not completely understood. The effects of the extraction conditions of (poly)phenols from fruits, before and after TT, on their antioxidant and antiglycation effects were assessed. (Poly)phenol-enriched extracts (PEEs) from raw and TT (90 °C, 1 h) were extracted using three solvent mixtures (ethanol/water/acetic acid) with increasing water content (0, 24, and 49%) and three solvent-to-solid ratios (5, 10, and 20 mL/g).

View Article and Find Full Text PDF
Article Synopsis
  • The study explores the use of pumpkin peels as a new source of eco-friendly pectin, utilizing a microwave-assisted extraction method with citric acid-acidified water.
  • Researchers optimized extraction conditions to achieve a pectin yield of 18.05%, finding high methoxyl content that classifies it as high methoxyl pectin, which has applications as a stabilizer and emulsifying agent.
  • The findings highlight the potential of utilizing agricultural waste for producing valuable polysaccharides, promoting sustainable practices and waste valorization in various industries.
View Article and Find Full Text PDF
Article Synopsis
  • Ferritin is an important protein for regulating iron metabolism in organisms and can be extracted from animal by-products for use in a circular economy.
  • A new method for extracting bovine liver ferritin (BLFer) using ultrasound-assisted techniques yields a higher output (32.18 g/kg) compared to traditional methods, while also enhancing structural stability.
  • The study finds that BLFer is a stable, hydrophilic protein that is crucial for iron management and has potential applications in food and other industries, promoting better use of animal by-products.
View Article and Find Full Text PDF

The present paper is a comprehensive study on the optimization of ultrasonic assisted extraction and characterization of valued components from the newly developed garlic cultivar NARC-G1. The response surface methodology was employed to optimize the extraction time, solvent-to-solid ratio and extraction temperature, for optimal total phenolic contents (TPC), DPPH radical scavenging activity, α-amylase inhibition, and α-glucosidase inhibition. Under the optimized conditions (23 min extraction time, 60 °C temperature, and 39 : 1 solvent-to-solute ratio) the optimal TPC (13.

View Article and Find Full Text PDF

Optimization of Phenolic-Enriched Extracts from Olive Leaves via Ball Milling-Assisted Extraction Using Response Surface Methodology.

Molecules

August 2024

Research and Development Department, Shanghai Chicmax Cosmetic Co., Ltd., 38th Floor, Global Harbor Tower B, No. 3300 North Zhongshan Road, Putuo District, Shanghai 200065, China.

This study aims to extract phenolic-enriched compounds, specifically oleuropein, luteoloside, and hydroxytyrosol, from olive leaves using ball milling-assisted extraction (BMAE). Response surface methodology (RSM) and the Box-Behnken design (BBD) were used to evaluate the effects of the temperature, solvent-to-solid ratio, and milling speed on extraction recovery. The contents of the extract were determined by ultra-high-performance liquid chromatography-mass spectrometry (UPLC-MS) and converted to recoveries to evaluate the extraction efficiency.

View Article and Find Full Text PDF

Want AI Summaries of new PubMed Abstracts delivered to your In-box?

Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!