A FAAS method was established for the determination of Na, K, Mg, Ca, Cu, Zn, Fe, Mn, Ni, Co, Pb, Cr, Cd, Ag and Au in Cynomorium songaricum after digestion with HNO3-HClO4 (phi 4:1) at 90-95 degrees C and at normal pressure. In this paper, the parameters in FAAS were studied. The analytical results of Na, K, Mg, Ca, Fe, Zn, Cu, Mn, Pb, Ni and Ag were 13,572.0, 14,260.0, 358.3, 168.3, 238.5, 19.4, 5.9, 3.4, 2.6, 1.3 and 0.4 microg x g(-1) respectively and Co, Cr, Cd and Au were not found in the samples. The results showed that the recovery of standard addition was 97.8%-104.5%, and the relative standard deviation (n = 9) was 0.2%-5.0%. The method is fast, simple and convenient. The results were satisfactory.
Download full-text PDF |
Source |
---|
Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!