Factors such as light-curing mode, filling technique and cavity configuration may affect the bonding strength to dentin. This study evaluated the effect of irradiation mode and filling technique on resin/dentin bonding strength on the buccal wall of Class I cavities in human teeth. Occlusal enamel was removed to expose a flat dentin surface. Occlusal cavities (4 x 3 x 3 mm) were prepared in dentin. The adhesive Single Bond was applied according to the manufacturer's instructions and TPH Spectrum composite resin was placed using the following: oblique incremental, horizontal incremental or bulk filling techniques. The composite resin was light-cured either by continuous (600 mW/cm2 for 40 s) or Soft-Start (250 mW/cm2 for 10 s + 600 mW/cm2 for 30 s) modes. Specimens of the control group were obtained by bonding the material to the flat exposed buccal wall of the cavity (C-factor = 1). The teeth were stored in water at 37 degrees C for 24 h and prepared for microtensile testing. Bonded beams of approximately 0.8 mm2 were obtained from the buccal wall and tested with a tension of 0.5 mm/min. Results were analyzed by two-way ANOVA, Tukey's test and Dunnett's test (alpha = 0.05). Incremental placement techniques with both irradiation modes produced higher bonding strength values than the bulk technique (p < 0.05). Bonding strength tested in the cavities had lower values than those obtained in flat dentin surfaces (control group) (p < 0.05), except for incremental fillings using stepped irradiation. Bonding strength to the cavity walls depends on the filling technique and on the irradiation mode of composite resins.
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http://dx.doi.org/10.1590/s1806-83242004000300015 | DOI Listing |
Int J Biol Macromol
January 2025
College of Chemistry, Beijing University of Chemical Technology, Beijing 100029, People's Republic of China. Electronic address:
The advancement of active packaging for food conservation has attracted considerable interest over time. In the present study, we aims to create and examine active films composed of chitosan (CS), poly(vinyl alcohol) (PVA), and syzygium guineense plant extract (SYZ) for potential use in food preservation. We examined the impact of ethanol extracts from the SYZ plant on the films' tensile strength, physical, antibacterial, and anti-oxidant properties.
View Article and Find Full Text PDFAngew Chem Int Ed Engl
January 2025
Shanghai Jiao Tong University, School of Chemistry and Chemical Engineering, 800 Dongchuan Road, 200240, Shanghai, CHINA.
Ionogels have attracted considerable attention as versatile materials due to their unique ionic conductivity and thermal stability. However, relatively weak mechanical performance of many existing ionogels has hindered their broader application. Herein, we develop robust, tough, and impact-resistant mechanically interlocked network ionogels (IGMINs) by incorporating ion liquids with mechanical bonds that can dissipate energy while maintain structural stability.
View Article and Find Full Text PDFBMC Oral Health
January 2025
Faculty of Dentistry, Department of Restorative Dentistry, Gazi University, Bişkek St. 1. St. Number: 8 Emek, Ankara, Turkey.
Background: Repairing composite resins is a less invasive alternative to complete restoration replacement. To achieve a successful bond between the existing and newly applied composite materials, various surface preparation methods, such as sandblasting and acid etching, have been explored. The aim of the study was to evaluate the effect of different surface treatments on the repair bond strength of a universal nanohybrid composite resin restorative material before and after thermal aging, by utilizing a micro-shear bond strength (µSBS) test.
View Article and Find Full Text PDFCarbohydr Polym
March 2025
College of Bioresources Chemical and Materials Engineering, Shaanxi University of Science and Technology, Shaanxi Provincial Key Laboratory of Papermaking Technology and Specialty Paper Development, Key Laboratory of Paper Based Functional Materials of China National Light Industry, National Demonstration Center for Experimental Light Chemistry Engineering Education, Xi'an 710021, China.
Current conventional wound dressings used for wound healing are often characterized by restricted bioactivity and devoid of multifunctionality resulting in suboptimal treatment and prolonged healing. Despite recent advances, the simultaneous incorporation of excellent flexibility, good mechanical performance, self-healing, bioactivity, and adhesion properties into the dressings without complicating their efficacy while maintaining simple synthesis remains a grand challenge. Herein, we effectively synthesized hybrid hydrogels of cellulose nanofiber (CNF), polyvinyl alcohol (PVA), and curcumin-modified silver nanoparticles (cAg) through a one-step synthesis method based on hydrogen bonds, dynamic boronic ester bonds, and coordinate covalent bonds.
View Article and Find Full Text PDFCarbohydr Polym
March 2025
Beijing Key Laboratory of Lignocellulosic Chemistry, Beijing Forestry University, Beijing 100083, China; State Key Laboratory of Efficient Production of Forest Resources, Beijing Forestry University, Beijing 100083, China. Electronic address:
Xylan-derived packaging materials have gained considerable popularity owing to their renewability, non-toxicity, and biodegradability. However, thermoforming is challenging owing to its rigid structure and hydrogen-bonding network of the xylan molecular chain, which limits its large-scale production. Herein, a heat-processable xylan derivative, xylan cinnamate (XC), was synthesized via an esterification reaction in ionic liquids.
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