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On-Demand Continuous Flow Synthesis of Pentafluorosulfanyl Chloride (SFCl) Using a Custom-Made Stirring Packed-Bed Reactor.
Chemistry
January 2025
Université de Montréal, FRQNT Centre in Green Chemistry and Catalysis, Centre for Continuous Flow Synthesis, Department of Chemistry, 1375 av. Thérèse Lavoie-Roux, Montréal, QC, H2V 0B3, Canada.
The pentafluorosulfanyl (SF-) group has been the subject of a surge of interest in the past decade, but there is still little practicality associated with its synthesis and installation. Herein is reported the first continuous flow synthesis of pentafluorosulfanyl chloride (SFCl), the most common reagent for the synthesis of SF-substituted compounds. The synthesis is based on inexpensive and easy-to-handle reagents: sulfur powder (S), trichloroisocyanuric acid (TCCA) and potassium fluoride (KF).
View Article and Find Full Text PDFEvaluation of microplate handling accuracy for applying robotic arms in laboratory automation.
SLAS Technol
December 2024
Artificial Intelligence Research Center, National Institute of Advanced Industrial Science and Technology, 2-4-7, Aomi, Tokyo, 135-0064, Japan; Laboratory for Biologically Inspired Computing, RIKEN Center for Biosystems Dynamics Research. 6-2-3 Furuedai, Suita, Osaka, 565-0874, Japan. Electronic address:
An inexpensive single-arm robot is widely utilized for recent laboratory automation solutions. The integration of a single-arm robot as a transfer system into a semi-automatic liquid dispenser without a transfer system can be realized as an inexpensive alternative to a fully automated liquid handling system. However, there has been no quantitative investigation of the positional accuracy of robot arms required to transfer microplates.
View Article and Find Full Text PDFFacile photopatterning of perfusable microchannels in hydrogels for microphysiological systems.
Nat Protoc
January 2025
George W. Woodruff School of Mechanical Engineering, Georgia Institute of Technology, Atlanta, GA, USA.
Perfusable hydrogels have garnered substantial attention in recent years for the fabrication of microphysiological systems. However, current methodologies to fabricate microchannels in hydrogel platforms involve sophisticated equipment and techniques, which hinder progress of the field. In this protocol, we present a cost-effective, simple, versatile and ultrafast method to create perfusable microchannels of complex shapes in photopolymerizable hydrogels.
View Article and Find Full Text PDFA New Method to Design and Manufacture a Low-Cost Custom-Made Template for Mandible Cut and Repositioning Using Standard Plates in BSSO Surgery.
Bioengineering (Basel)
June 2024
Department of Industrial Engineering, University of Salerno, Via Giovanni Paolo II, 132, 84084 Fisciano, SA, Italy.
In this study, a new methodology for designing and creating a custom-made template for maxillofacial surgery has been developed. The custom-made template can be used both for cutting and repositioning of the mandible arches for executing a BSSO (bilateral sagittal split osteotomy) treatment. The idea was developed in order to give the possibility of using a custom-made template with standard plates, thus reducing long times, high costs and low availability of custom-made plates; this represents the proof of novelty of the proposed template, based on a well-established methodology.
View Article and Find Full Text PDFEnhancing agricultural automation through weather invariant soil parameter prediction using machine learning.
Heliyon
April 2024
Department of Computer Science and Engineering, University of Dhaka, Dhaka, Bangladesh.
Soil parameters are crucial aspects in increasing agricultural production. Even though Bangladesh is heavily dependent on agriculture, little research has been done regarding its automation. And a vital aspect of agricultural automation is predicting soil parameters.
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