The aim of this study was to evaluate the glass ionomer cement Ketac-Endo (K) compared with Endofill (E), N-Rickert (N), and Sealer 26 (S) in terms of disintegration, solubility, and dimensional alteration properties, based on ADA Specification No 57. For dimensional alterations, 12-mm high cylindric specimens measuring 6 mm in diameter were prepared and left to stand for a period corresponding to three times the setting time. These specimens were immersed in 30 ml of deionized distilled water after measuring their length with a caliper. Thirty days later, the sample was removed from the container, dried and measured again for length to determine the percent of dimensional alteration. For solubility and disintegration, 1.5-mm thick cement samples measuring 20 mm in diameter were prepared and left to stand for a period corresponding to three times the setting time. The samples were weighed and immersed in 50 ml of deionized distilled water. After seven days, the samples were removed, dried and weighed again to determine the mass loss of each sample, expressed as percentage of original mass. This was considered to correspond to solubility and disintegration of cement. The results were: dimensional alteration: E (+0.14), K (-0.24), N (+0.23), S (+3.26); for disintegration and solubility: E (3.90), K (9.90), N (3.00), S (0.25). We concluded that the dimensional alteration of all cements conformed to ADA standards; Endofill and Ketac-Endo sealers presented higher values for disintegration and solubility than ADA recommendations. Obturating a root canal with a sealer that presents low disintegration and low contraction could minimize the penetration of fluids into the root canal system, thus sealing the space hermetically.
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http://dx.doi.org/10.1590/s0103-64402003000200008 | DOI Listing |
Spectrochim Acta A Mol Biomol Spectrosc
December 2024
School of Chemistry and Chemical Engineering, Nanchang University, Nanchang 330031, Jiangxi, China. Electronic address:
Apo-transferrin (apo-TRF) is a vital protein for maintaining iron balance in the body, which is produced by the liver. Indisulam (IDM) has been extensively used to treat cancer in clinical study and has been identified as a molecular glue. Iron imbalances in the body are believed to encourage the growth and spread of cancer cells.
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December 2024
Université de Lorraine, CNRS, LIEC, F-54000, Nancy, France.
There is a growing interest in the development of methods for the detection of nanoparticle (NP) toxicity to living organisms based on the analysis of relevant multidimensional data sets. In particular the detection of preliminary signs of NPs toxicity effects would benefit from the selection of data featuring NPs-induced alterations of biological barriers. Accordingly, we present an original Topological Data Analysis (TDA) of the nanomechanical properties of Escherichia coli cell surface, evaluated by multiparametric Atomic Force Microscopy (AFM) after exposure of the cells to increasing concentrations of titanium dioxide nanoparticles (TiONPs).
View Article and Find Full Text PDFFront Biosci (Landmark Ed)
November 2024
Department of General Surgery, The First Affiliated Hospital of Anhui Medical University, 230022 Hefei, Anhui, China.
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View Article and Find Full Text PDFForensic Sci Int
December 2024
Department of Forest Products and Biotechnology, Kookmin University, 77 Jeongneung-ro, Seongbuk-gu, Seoul 02707, Republic of Korea. Electronic address:
Paper differentiation can play a critical role in forensic document examination along with examinations of handwriting identification, impressed writing, and ink and printer toner analyses. If reference database to compare was constructed, paper analyses are also useful in terms of examining when document paper was produced. In this study, two datasets were utilized for principal component analysis (PCA) and t-SNE, and each dataset was constructed for the manufacturer discrimination and document paper dating tasks.
View Article and Find Full Text PDFJ Food Sci
December 2024
Food Science and Human Nutrition, University of Illinois at Urbana-Champaign, Urbana, Illinois, USA.
Microstructural properties of wheat-based food materials change during baking. These alterations affect the final product's mechanical properties, physical attributes, and consumer satisfaction. Image processing and pore network modeling were used to analyze the variations in a cookie's microstructural properties during baking.
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