The reaction between the lithium 3-sila-beta-diketiminate (1) and the appropriate MOBut yielded the crystalline sodium (2) or potassium (3) 3-sila-beta-diketiminate in high yield; X-ray crystal data and NMR spectra show new coordination modes for the [N(R)C(Ar)Si(R)C(Ar)N(R)]- ligand (R = SiMe3, Ar = C6H3Me(2)-2,6).
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| http://dx.doi.org/10.1039/b110443h | DOI Listing |
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