Crystals of caesium molybdenomethylenediphosphonate, [CsMoO(2)(CH(3)O(6)P(2))], were hydrothermally synthesized at 473 K. The monoclinic structure, as determined from single-crystal X-ray diffraction, is two-dimensional and consists of stacked mixed layers of corner-sharing tetrahedral diphosphonate groups and MoO(6) octahedra, between which Cs+ cations are intercalated.
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