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Heterogeneous allylsilylation of aromatic and aliphatic alkenes catalyzed by proton-exchanged montmorillonite.
Org Lett
April 2010
Graduate School of Science and Engineering, Tokyo Institute of Technology, 4259 Nagatsuta-cho, Midori-ku, Yokohama, 226-8502, Japan.
Allylsilylation of an alkene is the only known procedure to install both silyl and allyl groups onto a carbon-carbon double bond directly. Proton-exchanged montmorillonite showed excellent catalytic performances for the allylsilylation of alkenes. For example, the reaction of p-chlorostyrene with allyltrimethylsilane proceeded smoothly to afford the corresponding allylsilylated product in 95% yield.
View Article and Find Full Text PDFAllylsilylation of Carbon-Carbon and Carbon-Oxygen Unsaturated Bonds via a Radical Process(1).
J Org Chem
August 1998
Department of Chemistry, University of Tsukuba Tsukuba, Ibaraki 305-8571, Japan.
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