This study examined the relationship between mercury content and mercury evaporation from amalgams during setting. Two different types of commercial high-copper amalgams (single composition and admixed types) were used. Cylindrical specimens of each amalgam were prepared with five different mercury contents according to ADA Specification No.1. Specimens were also prepared by hand condensation. Mercury evaporation from amalgam specimens maintained at 37 degrees C was measured using a gold film mercury analyzer from 10 min after the end of trituration until the mercury concentration in air reached an undetectable level. The mercury content more clearly influenced the mercury evaporation from the admixed type amalgam specimens when the mercury content decreased below the manufacturers' recommended trituration conditions. Triturating with less mercury than the manufacturers' recommended amount cannot lower the evaporation of mercury from freshly made amalgam. Proper condensing procedures can minimize the mercury evaporation from the amalgam surface.
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http://dx.doi.org/10.4012/dmj.19.211 | DOI Listing |
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December 2024
Thin Film and NanoScience Laboratory, Department of Physics, Jadavpur University, Kolkata, 700032, India.
Acta Crystallogr B Struct Sci Cryst Eng Mater
June 2024
Institute of Low Temperature and Structure Research, Polish Academy of Sciences, Okólna 2, 50-950 Wrocław, Poland.
A new Zn coordination polymer (CP) based on 2,3-pyrazine dicarboxylic acid (Hpzdc) and 4,4'-bipyridine (bpy) (ZCP) was synthesized using a facile slow evaporation method. Single-crystal X-ray diffraction revealed that ZCP is a two-dimensional porous CP, [Zn(pzdc)(bpy)(HO)], with van der Waals forces as the dominant interaction within its layers forming a 6 network. Employing energetic ultrasound irradiation, nanoscale ZCP (nZCP) was successfully synthesized and Eu ions were incorporated within its host lattice (Eu@nZCP).
View Article and Find Full Text PDFMaterials (Basel)
April 2024
Department of Mechanical Engineering, North Carolina A & T State University, Greensboro, NC 27411, USA.
Dental amalgams have been used by dentists for the restoration of posterior human teeth. However, there have been concerns about the release of mercury from amalgams into the oral cavity. The objective of the present research is to study the effect of titanium (Ti) nanoparticles on the microstructural mechanism of the release of mercury vapor in two commonly used brands of dental amalgam (the Dispersalloy: 11.
View Article and Find Full Text PDFMolecules
March 2024
Key Laboratory of Advanced Materials of Ministry of Education, Department of Chemical Engineering, Tsinghua University, Beijing 100084, China.
Polysilsesquioxane (PSQ) microspheres have shown promise in many fields, but previous studies about porous PSQ microspheres are scarce. Herein, we fabricated novel micron-sized thiol-functional polysilsesquioxane (TMPSQ) microspheres with open and interconnected macropores by combining inverse suspension polymerization with two-step sol-gel and polymerization-induced phase separation processes, without using phase-separation-promoting additives or sacrificial templates. The chemical composition of the TMPSQ microspheres was confirmed using FTIR and Raman spectroscopy.
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March 2024
Laboratory of Spectroscopic Characterizations and Optics Materials, University of Sfax, Faculty of Sciences of Sfax B. P. 1171 3000 Sfax Tunisia.
There has been a lot of interest in the development of a novel hybrid material based on mercury that has fascinating structural properties. In this paper, single crystals of [CHNO]HgBr was successfully synthesized by the slow evaporation method at room temperature. In fact, the latter crystallizes in the orthorhombic system ( space group) with cell parameters = 20.
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