Severity: Warning
Message: file_get_contents(https://...@pubfacts.com&api_key=b8daa3ad693db53b1410957c26c9a51b4908&a=1): Failed to open stream: HTTP request failed! HTTP/1.1 429 Too Many Requests
Filename: helpers/my_audit_helper.php
Line Number: 176
Backtrace:
File: /var/www/html/application/helpers/my_audit_helper.php
Line: 176
Function: file_get_contents
File: /var/www/html/application/helpers/my_audit_helper.php
Line: 250
Function: simplexml_load_file_from_url
File: /var/www/html/application/helpers/my_audit_helper.php
Line: 3122
Function: getPubMedXML
File: /var/www/html/application/controllers/Detail.php
Line: 575
Function: pubMedSearch_Global
File: /var/www/html/application/controllers/Detail.php
Line: 489
Function: pubMedGetRelatedKeyword
File: /var/www/html/index.php
Line: 316
Function: require_once
The development and application of a solid-phase microextraction (SPME) method in the analysis of vanilla extracts and vanilla flavorings was studied. The SPME method was developed to be used in conjunction with gas chromatography mass spectrometry (GC-MS). The optimized SPME sampling parameters for the determination of the volatile components included a poly(acrylate) fiber, a 40-min sampling time at room temperature, and a 2-min desorption time. The reproducibility of the method was good, with a percent relative standard deviation between 2.5 and 6.4% for the target compounds. The data suggest that the origin of natural extracts can be readily determined from the GC profile and that differences exist between nature-identical and synthetic flavorings and the natural extracts. The method also has potential for identifying the type of vanilla extract/flavoring used to flavor food.
Download full-text PDF |
Source |
---|---|
http://dx.doi.org/10.1021/jf000515+ | DOI Listing |
Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!