Improvement of photocatalytic degradation of methyl orange by impregnation of natural clay with nickel: optimization using the Box-Behnken design (BBD).

In this research work, the photocatalytic degradation of methyl orange dye was studied on nickel oxide supported on a natural Moroccan clay (Ni/NC). These catalysts have been prepared by dry impregnation of a nickel nitrate solution with different weight percentages (5, 10, 20% NiO). Experimental responses were obtained by a Box-Behnken (BBD) experimental design by varying the catalyst mass, solution pH, and initial dye concentration at three levels (low, medium, and high).