In the field of quantitative X-ray analysis techniques, such as electron probe microanalysis, precise knowledge of fundamental parameters is crucial. Especially, the accurate determination of photon mass attenuation coefficients is essential to perform correct elemental quantification. While the widely used databases offer agreement for the hard X-ray range, significant differences arise for lower photon energies.
View Article and Find Full Text PDFA cryogenic electrical-substitution radiometer was used for the primary calibration of monochromatic photon beams at synchrotron, which are in turn employed to determine the intrinsic efficiency of an HPGe detector between 3.5 keV and 8 keV. This allowed the determination of the thickness of the dead layer, which enabled the calculation of the efficiency up to 55 keV, where the active thickness is not determinant.
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