We have prepared CuO-derived electrocatalysts on a graphitic carbon nitride (-CN) nanosheet support for the electrochemical carbon dioxide reduction reaction (CORR). Highly monodisperse CuO nanocrystals made by a modified colloidal synthesis method serve as the precatalysts. We use a two-stage thermal treatment to address the active site blockage issues caused by the residual C18 capping agents.
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