Influence of processing conditions on bioactive compound extraction from L. var. Alicante Bouschet grape skin.

The aim of this study was to evaluate the effects of process conditions on the solid-liquid extraction of bioactive compounds from the Alicante Bouschet grape skin from the semi-arid region of Brazil. The influence of temperature (23-57 °C), ethanol concentration (16-84%) and citric acid concentration (0-4%) on the total phenolic content, monomeric anthocyanin content and on the antioxidant capacity of the extracts measured by oxygen radical absorbance capacity and cation radical scavenging activity (ABTS) methods was investigated. Ethanol concentration and temperature had a significant influence on total phenolic compounds extraction and antioxidant capacity while monomeric anthocyanins extraction was only affected by ethanol concentration.

Development and validation of a gas chromatographic method by solid-phase microextraction for the determination of surface flavouring content in encapsulated flavouring.

A solid-phase microextraction procedure followed by analysis by gas chromatography is proposed to determine surface flavouring content in encapsulated flavouring. The method showed a good selectivity, as well as good intraday and interday precision, CVs<4% in both cases. The calibration curves were linear at the tested ranges (R=0.