The present work showed the green, eco-friendly synthesis of zinc oxide nanoparticles (ZnO NPs) using leaf extract of Cucurbita pepo. The prepared ZnO NPs were studied using different characterization techniques such as Fourier transform infrared (FTIR), X-ray diffraction (XRD), UV-Visible spectroscopy (UV-Vis) and Transmission electron microscopy (TEM). TEM images confirmed the formation of NPs with average size of 8 nm.
View Article and Find Full Text PDFGuang Pu Xue Yu Guang Pu Fen Xi
January 2010
Five different sample solvents (trifluoroacetic acid, tetrahydrofuran, formic acid, acetonitrile, 60% acetonitrile /5% trifluoroacetic acid) and two kinds of sample preparation methods were chosen for characterizing the structure, mole mass and mass distribution of insoluble polymer of polyamide-6, T (PA6T) by matrix assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS). It was shown that the spectra with wide mole mass and high signal-to-noise (S/N) ratio were obtained, when using 60% acetonitrile /5% trifluoroacetic acid as solvent, and solvent sample preparation with one step droplet method was better than non-solvent sample preparation. The main chain structure of PA6T polymerized in ionic liquid was analyzed, which was linear without the presence of cyclic polymer.
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