Clinoptilolite based zeolite-geopolymer foams (abbreviated as CFs) were prepared from natural clinoptilolite and calcined clinoptilolite, using HO solution as pore former through a straightforward process. Natural clinoptilolite and CFs are characterized by analytical techniques including optical microscope, XRF, FTIR, XRD, BET, MIP and SEM. The obtained CFs possesses micropores of zeolite and meso/macropores of geopolymer matrix.
View Article and Find Full Text PDFPolypropylene-based cerium wet catalytic materials (Ce/PPNW--PAA) were prepared through ultraviolet grafting and ion exchange technology. They were used as effective and reusable heterogeneous catalysts for rhodamine B (RhB) degradation. The physicochemical properties of Ce/PPNW--PAA were characterized by Fourier transform infrared (FT-IR) spectroscopy, scanning electron microscopy (SEM), specific surface area measurements (BET), and X-ray photoelectron spectroscopy (XPS).
View Article and Find Full Text PDFThe analysis of siliceous matrix samples may adopt a two-step pretreatment, which includes melting with ammonium hydrogen fluoride and redissolving with nitric acid. However, the residual of substrate silicon unfavorable to the determination of trace elements in the samples due to serious matrix effects. Here, a new digestion method using simultaneously both ammonium bifluoride and nitric acid under normal pressure was developed for high-purity quartz sand sample.
View Article and Find Full Text PDF